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Identification and imaging of modern paints using Secondary Ion Mass Spectrometry with MeV ions

Bogdanović Radović, Ivančica; Siketić, Zdravko; Jembrih- Simbürger, Dubravka; Marković, Nikola; Anghelone, Marta; Stoytschew, Valentin; Jakšić, Milko (2017) Identification and imaging of modern paints using Secondary Ion Mass Spectrometry with MeV ions. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 406 (Part A). pp. 296-301. ISSN 0168-583X

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Abstract

Secondary Ion Mass Spectrometry using MeV ion excitation was applied to analyse modern paint materials containing synthetic organic pigments and binders. It was demonstrated that synthetic organic pigments and binder components with molecular masses in the m/z range from 1 to 1200 could be identified in different paint samples with a high efficiency and in a single measurement. Different ways of mounting of mostly insulating paint samples were tested prior to the analysis in order to achieve the highest possible yield of pigment main molecular ions. As Time-of-Flight mass spectrometer for MeV Secondary Ion Mass Spectrometry is attached to the heavy ion microprobe, molecular imaging on cross- sections of small paint fragments was performed using focused ions. Due to the fact that molecules are extracted from the uppermost layer of the sample and to avoid surface contamination, the paint samples were not embedded in the resin as is usually done when imaging of paint samples using different techniques in the field of cultural heritage.

Item Type: Article
Uncontrolled Keywords: MeV-SIMS ; synthetic organic pigments ; modern paints ; heavy ion microprobe ; molecular imaging
Subjects: NATURAL SCIENCES > Physics
Divisions: Division of Experimental Physics
Depositing User: Ivančica Bogdanović Radović
Date Deposited: 25 Aug 2017 13:18
Last Modified: 28 Aug 2017 12:17
URI: http://fulir.irb.hr/id/eprint/3542
DOI: 10.1016/j.nimb.2017.01.007

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